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    2. ASTM F467 Grade R52400

    ASTM F467/F467M Grade R52400 Alloy 7 Nuts Specification

    Titanium alloy nuts manufactured for superior corrosion resistance.

    ASTM F467/F467M Grade R52400 Alloy 7 Nuts are widely used in chemical processing and marine industries because of their excellent resistance to corrosion and oxidation.

    ASTM F467/F467M Chemical Composition

    ASTM F467/F467M Titanium and Titanium-Base Alloys A

    UNS Designation Number Alloy General Name Al C Fe Ti H N O Pd V Cr Mo Zr Sn Si Ru Residuals B
    each, max total, max
    ASTM F467/F467M Grade R52400 7 Titanium Gr 7 . . . 0.10 0.30 balance 0.0125 0.05 0.25 0.12- 0.25 . . . . . . . . . . . . . . . . . . . . . 0.1 0.4
    • (A) All reported values are maximums, unless a range is specified.
    • (B) A residual is an element present in a metal or an alloy in small quantities inherent to the manufacturing process but not added intentionally. Residual elements need not be reported unless a report is specifically required by the purchaser.
    • (C) Ruthenium and Palladium, or both, may be added to Grade 19 for enhanced corrosion resistance as negotiated between purchaser and vendor. Chemical analysis is not required unless specifically negotiated.

    ASTM F467/F467M Mechanical Requirements

    ASTM F467/F467M Mechanical Requirements (Inch)

    Alloy Mechanical Property Marking Hardness, min A Proof Stress, Hex Nut min, ksi Proof Stress, Heavy Hex Nut min, ksi B
    ASTM F467 Alloy Ti 7 F 467ET 160 HV 55 59
    • (A) For aluminum and titanium alloys hardness values are for information only.
    • (B) Proof stress values for heavy hex nuts are based on 1.08 times the value for corresponding regular hex nuts.
    • (C) Aluminum alloy 2024-T4 shall be supplied in naturally aged condition. This material is not recommended for nuts in sizes greater than 1/4 (0.250) in.

    ASTM F467M Mechanical Requirements (Metric)

    Alloy Mechanical Property Marking Hardness, min A Proof Stress, Mpa
    ASTM F467M Ti 7 F467MET 160 HV 380
    • (A) For aluminum and titanium alloys hardness values are for information only.
    • (B) Aluminum alloy 2024-T4 shall be supplied in naturally aged condition. This material is not recommended for nuts in nominal thread diameter larger than M6.

    ASTM F467/F467M Tensile Stress Areas and Threads per Inch

    Nominal Size, in. Coarse Threads-UNC Fine Threads-UNF 8 Thread Series-8UN
    Threads/in. Stress Area A, in 2 Threads/in. Stress Area A, in 2 Threads/in. Stress Area A, in 2
    1/ 4 20 0.0318 28 0.0364 . . . . . .
    5/ 16 18 0.0524 24 0.0580 . . . . . .
    3/ 8 16 0.0775 24 0.0878 . . . . . .
    7/ 16 14 0.1063 20 0.1187 . . . . . .
    1/ 2 13 0.1419 20 0.1599 . . . . . .
    9/ 16 12 0.1820 18 0.2030 . . . . . .
    5/ 8 11 0.2260 18 0.2560 . . . . . .
    3/ 4 10 0.3340 16 0.3730 . . . . . .
    7/ 8 9 0.4620 14 0.5090 . . . . . .
    1 8 0.6060 12 0.6630 . . . . . .
    1 1/ 8 7 0.7630 12 0.8560 8 0.790
    1 1/ 4 7 0.9690 12 1.0730 8 1.000
    1 3/ 8 6 1.1550 12 1.3150 8 1.233
    1 1/ 2 6 1.4050 12 1.5810 8 1.492
    • (A) Tensile stress areas are computed using the following formula:
    • A s = 0.7854 [ D - 0.9743/n ]
      • where:
      • As = tensile stress area, in. 2 ,
      • D = nominal size (basic major diameter), in., and
      • n = number of threads per inch.

    ASTM F467/F467M Tensile Stress Areas and Threads per Metric

    Nominal Nut Diameter and Thread Pitch Stress Area, Amm 2 Nominal Nut Diameter and Thread Pitch Stress Area, Amm 2
    M6 × 1 20.1 M16 × 2 157
    M8 × 1.25 36.6 M20 × 2.5 245
    M10 × 1.5 58.0 M24 × 3 353
    M12 × 1.75 84.3 M30 × 3.5 561
    M14 × 2 115 M36 × 4 817
    • (A) Tensile stress areas are computed using the following formula:
    • As = 0.7854 (D − 0.9382P) 2
      • where:
      • As = tensile stress area, mm. 2 ,
      • D = nominal size (basic major diameter), mm., and
      • n = number of threads per mm.

    ASTM F467/F467M Heat Treatment

    Alloy Condition
    Copper (all alloys) As formed or stress relieved at manufacturer's option
    Nickel alloys 400 and 405 As formed or stress relieved at manufacturer's option
    Nickel alloy 500 Solution annealed and aged
    Aluminum alloy 2024-T4 Solution treated and naturally aged
    Aluminum alloy 6061-T6 Solution treated and artificially aged
    Aluminum alloy 6262-T9 Solution treated, artificially aged, and cold worked
    Titanium 625 Annealed

    Frequently Asked Questions

    What is Titanium Grade 7 (R52400)?

    Grade 7 is commercially-pure titanium with 0.12-0.25% palladium added per ASTM F467 - the Pd dramatically extends acceptable service into hot reducing acids (HCl, H2SO4, formic, oxalic) where unalloyed CP titanium would corrode. Tensile 50 ksi min, yield 40 ksi (similar to Grade 2).

    When do I need Grade 7 over Grade 2 titanium?

    Whenever service includes hot reducing acids, dilute reducing acids at elevated temperature, or any chemistry where CP titanium passive-film breakdown is a risk. Common applications: hydrochloric acid plants, phosphoric acid evaporators, pharmaceutical reactors using reducing solvents.

    Is the Pd addition cost-prohibitive?

    Palladium content is small (0.12-0.25%) but it dominates raw-material cost - Grade 7 nut typically runs 2-3x the price of Grade 2. For service that requires it, the cost is fully justified by avoided corrosion failures.

    Sour-service acceptance?

    Yes - R52400 is NACE MR0175-listed.

    References & Standards

    • ASTM F467 / F467M - Standard Specification for Nonferrous Nuts for General Use
    • ASTM F468 / F468M - Companion specification for Nonferrous Bolts, Hex Cap Screws, and Studs (mate with F467 nuts for matched-alloy assemblies)
    • ASTM F436 / F436M - Hardened steel washers (ferrous washer companion when nonferrous washers are not specified)
    • NACE MR0175 / ISO 15156 - Sour-service hardness limits for petroleum and natural gas industries
    • ASME B18.2.2 / B18.2.4.1M / B18.2.4.6M and ISO 4032 / 4033 / 4035 - Dimensional standards referenced by F467
    • DIN 934 / 439 / 6330 - Metric hex nut dimensional standards
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